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Information card for entry 7011506
Preview
Coordinates | 7011506.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C48 H63 Cl Ir2 N2 O6 S6 |
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Calculated formula | C48 H63 Cl Ir2 N2 O6 S6 |
Title of publication | Nucleophilic addition and substitution reactions on the sulfur atoms bound to two Ir atoms. Conversion of a hydrosulfido complex [(??5-C5Me5)2Ir2(??-SH)3]Cl into a series of diiridium complexes with bridging thiolato ligands |
Authors of publication | Takagi, Fusao; Seino, Hidetake; Hidai, Masanobu; Mizobe, Yasushi |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2002 |
Journal issue | 18 |
Pages of publication | 3603 |
a | 11.943 ± 0.002 Å |
b | 22.055 ± 0.002 Å |
c | 20.508 ± 0.002 Å |
α | 90° |
β | 90.01 ± 0.01° |
γ | 90° |
Cell volume | 5401.9 ± 1.2 Å3 |
Cell temperature | 296.2 K |
Ambient diffraction temperature | 296.2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0353 |
Residual factor for significantly intense reflections | 0.0353 |
Weighted residual factors for significantly intense reflections | 0.0364 |
Weighted residual factors for all reflections included in the refinement | 0.0364 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.349 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7011506.html
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