Information card for entry 7011552

Structure parameters

• Formula: C80 H116 Cu2 N24 O24
• Calculated formula: C20 H21 Cu0.5 N6 O6
• Title of publication: Assembly of supermolecular complexes with tripodal ligand titmb and tib: a 2D rhombic grid network assembled from 2-connected tib
• Authors of publication: Liu, Hong-Ke; Sun, Wei-Yin; Tang, Wen-Xia; Tan, Hai-Yan; Zhang, Hua-Xin; Tong, Ye-Xiang; Yu, Xiao-Lan; Kang, Bei-Sheng
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 20
• Pages of publication: 3886
• a: 10.565 ± 0.002 Å
• b: 12.13 ± 0.002 Å
• c: 17.726 ± 0.004 Å
• α: 90°
• β: 103.72 ± 0.03°
• γ: 90°
• Cell volume: 2206.8 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1509
• Residual factor for significantly intense reflections: 0.081
• Weighted residual factors for significantly intense reflections: 0.2218
• Weighted residual factors for all reflections included in the refinement: 0.2686
• Goodness-of-fit parameter for all reflections included in the refinement: 0.993
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No