Crystallography Open Database

Information card for entry 7011676

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Coordinates	7011676.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C62 H78 N4 Ni
Calculated formula	C53 H74 N3 Ni0.5
Title of publication	First-row transition metal complexes of sterically-hindered amidinates
Authors of publication	Schmidt, Joseph A. R.; Arnold, John
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	18
Pages of publication	3454
a	12.459 ± 0.0009 Å
b	15.941 ± 0.001 Å
c	14.07 ± 0.001 Å
α	90°
β	105.396 ± 0.001°
γ	90°
Cell volume	2694.1 ± 0.3 Å³
Cell temperature	193.2 K
Ambient diffraction temperature	193.2 K
Number of distinct elements	4
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.062
Residual factor for significantly intense reflections	0.0347
Weighted residual factors for significantly intense reflections	0.041
Weighted residual factors for all reflections included in the refinement	0.041
Goodness-of-fit parameter for all reflections included in the refinement	1.373
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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