Information card for entry 7011698

Structure parameters

• Formula: C19 H55 Cl4 Cu3 N9 O21
• Calculated formula: C19 H55 Cl4 Cu3 N9 O21
• Title of publication: Solvent controlled nuclearity in Cu(ii) complexes linked by the CO32− ligand: synthesis, structure and magnetic properties
• Authors of publication: Rodríguez, Montserrat; Llobet, Antoni; Corbella, Montserrat; Müller, Peter; Usón, Miguel Angel; Martell, Arthur E.; Reibenspies, Joseph
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 14
• Pages of publication: 2900
• a: 22.664 ± 0.005 Å
• b: 21.033 ± 0.004 Å
• c: 17.55 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8366 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0181
• Residual factor for significantly intense reflections: 0.0121
• Weighted residual factors for significantly intense reflections: 0.0281
• Weighted residual factors for all reflections included in the refinement: 0.0282
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No