Information card for entry 7011792

Structure parameters

• Chemical name: hexakis-(dimethylsulfoxide)-nickel(II) tetrachloronickelate(II)
• Formula: C12 H36 Cl4 Ni2 O6 S6
• Calculated formula: C12 H36 Cl4 Ni2 O6 S6
• Title of publication: Reactivity of five- and six-coordinated solvates. A complex formation and crystallographic study of the nickel(II) bromide and iodide systems in dimethyl sulfoxide and N,N'-dimethylpropyleneurea
• Authors of publication: Bobicz, Dorota; Kristiansson, Olof; Persson, Ingmar
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 22
• Pages of publication: 4201 - 4205
• a: 18.95 ± 0.002 Å
• b: 18.95 ± 0.002 Å
• c: 8.5688 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3077.1 ± 0.7 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 85
• Hermann-Mauguin space group symbol: P 4/n :2
• Hall space group symbol: -P 4a
• Residual factor for all reflections: 0.1357
• Residual factor for significantly intense reflections: 0.0546
• Weighted residual factors for significantly intense reflections: 0.1348
• Weighted residual factors for all reflections included in the refinement: 0.1531
• Goodness-of-fit parameter for all reflections included in the refinement: 0.967
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No