Structure and vibrational properties of ethyltrioxorhenium(vii), C2H5ReO3, investigated by gas electron diffraction, single crystal X-ray diffraction, IR spectroscopy and quantum chemical calculations
Authors of publication
Downs, Anthony J.; Geisberger, Martin R.; Green, Jennifer C.; Greene, Tim M.; Haaland, Arne; Herrmann, Wolfgang A.; Morris, Leigh J.; Parsons, Simon; Scherer, Wolfgang; Volden, Hans Vidar
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
2002
Journal issue
17
Pages of publication
3342
a
6.421 ± 0.003 Å
b
5.111 ± 0.002 Å
c
15.108 ± 0.005 Å
α
90°
β
98.01 ± 0.04°
γ
90°
Cell volume
491 ± 0.3 Å3
Cell temperature
150 K
Ambient diffraction temperature
150 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for significantly intense reflections
0.0406
Weighted residual factors for all reflections included in the refinement
0.0435
Goodness-of-fit parameter for all reflections included in the refinement