Information card for entry 7011828

Structure parameters

• Formula: C30 H49 As6 B2 F8 Fe O0.5
• Calculated formula: C30 H49 As6 B2 F8 Fe O0.5
• Title of publication: Homoleptic iron(II)–diphosphine and –diarsine complexes: syntheses, characterization and redox properties
• Authors of publication: Annemarie A. La Pensée; Jamie Bickley; Simon J. Higgins
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 16
• Pages of publication: 3241 - 3244
• a: 12.0709 ± 0.0007 Å
• b: 16.5127 ± 0.0009 Å
• c: 38.986 ± 0.002 Å
• α: 90°
• β: 95.535 ± 0.001°
• γ: 90°
• Cell volume: 7734.6 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0532
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.0811
• Weighted residual factors for all reflections included in the refinement: 0.0872
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No