Information card for entry 7011835

Structure parameters

• Formula: C48.33 H40 Cl4.67 N12 O8.67 Ru2
• Calculated formula: C48.3333 H38 Cl4.66667 N12 O8.66667 Ru2
• Title of publication: Dinuclear ruthenium(ii) complexes [{(L)ClRuII}2(??-tppz)]2+ (L = an arylazopyridine ligand) incorporating tetrakis(2-pyridyl)pyrazine (tppz) bridging ligand: synthesis, structure and spectroelectrochemical properties
• Authors of publication: Chanda, Nripen; Laye, Rebecca H.; Chakraborty, Soma; Paul, Rowena L.; Jeffery, John C.; Ward, Michael D.; Lahiri, Goutam Kumar
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 18
• Pages of publication: 3496
• a: 10.9908 ± 0.0003 Å
• b: 12.7354 ± 0.0003 Å
• c: 27.5708 ± 0.0007 Å
• α: 98.012 ± 0.002°
• β: 96.645 ± 0.001°
• γ: 99.56 ± 0.002°
• Cell volume: 3730.11 ± 0.17 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0702
• Residual factor for significantly intense reflections: 0.0566
• Weighted residual factors for significantly intense reflections: 0.1593
• Weighted residual factors for all reflections included in the refinement: 0.2097
• Goodness-of-fit parameter for all reflections included in the refinement: 1.129
• Diffraction radiation wavelength: 1.54056 Å
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No