Crystallography Open Database

Information card for entry 7011843

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Coordinates	7011843.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H5 Co2 N O6
Calculated formula	C14 H5 Co2 N O6
Title of publication	A novel approach to the synthesis of azobenzene using dicobalt carbonyl
Authors of publication	Hong, Fung-E; Chen, Cheng-Wei; Chang, Yu-Chang
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	15
Pages of publication	2951
a	8.2979 ± 0.0006 Å
b	9.6328 ± 0.0008 Å
c	9.784 ± 0.0008 Å
α	78.95 ± 0.002°
β	75.756 ± 0.002°
γ	88.829 ± 0.002°
Cell volume	743.66 ± 0.1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0436
Residual factor for significantly intense reflections	0.0363
Weighted residual factors for significantly intense reflections	0.1026
Weighted residual factors for all reflections included in the refinement	0.1101
Goodness-of-fit parameter for all reflections included in the refinement	0.851
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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