Crystallography Open Database

Information card for entry 7012019

7012018 << 7012019 >> 7012020

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Coordinates	7012019.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74 H86 N5 Nd O19 P4
Calculated formula	C74 H86 N5 Nd O19 P4
Title of publication	Synthesis and coordination chemistry of arene soluble 4-alkyl-2,6-bis[(diphenylphosphino)methyl]pyridine N,P,P'-trioxide ligands
Authors of publication	Xin-Min Gan; Robert T. Paine; Eileen N. Duesler; Heinrich Nöth
Journal of publication	Dalton Trans.
Year of publication	2003
Journal issue	1
Pages of publication	153 - 159
a	13.2909 ± 0.0008 Å
b	14.9667 ± 0.0009 Å
c	20.0288 ± 0.0011 Å
α	86.494 ± 0.001°
β	79.813 ± 0.001°
γ	83.38 ± 0.001°
Cell volume	3891.8 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0564
Residual factor for significantly intense reflections	0.0457
Weighted residual factors for significantly intense reflections	0.1292
Weighted residual factors for all reflections included in the refinement	0.1363
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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