Crystallography Open Database

Information card for entry 7012034

7012033 << 7012034 >> 7012035

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Coordinates	7012034.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51 H42 Cl3 O2.5 P2 Ru
Calculated formula	C51 H39 Cl3 O2.5 P2 Ru
Title of publication	Synthesis and derivatization, structures and transition metal chemistry of a new large bite bis(phosphinite) derived from bis(2-hydroxy-1-naphthyl)methane
Authors of publication	Balakrishna, Maravanji S.; Panda, Rashmishree; Mague, Joel T.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	24
Pages of publication	4617
a	41.312 ± 0.002 Å
b	12.8234 ± 0.0017 Å
c	22.77 ± 0.002 Å
α	90°
β	122.897 ± 0.008°
γ	90°
Cell volume	10128.4 ± 1.9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1585
Residual factor for significantly intense reflections	0.0619
Weighted residual factors for significantly intense reflections	0.1947
Weighted residual factors for all reflections included in the refinement	0.2354
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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