Information card for entry 7012054

Structure parameters

• Formula: Al H28 La Mo6 O35
• Calculated formula: Al La Mo6 O35
• Title of publication: A novel polyoxometalate chain formed from heteropolyanion building blocks and rare earth metal ion linkers: [La(H2O)7Al(OH)6Mo6O18]n??4nH2OElectronic supplementary information (ESI) available: representations of the structure of 1 with the atom numbering scheme and hydrogen bonding interactions shown and a list of relevant hydrogen bonding distances. See http://www.rsc.org/suppdata/dt/b2/b207149e/
• Authors of publication: Shivaiah, Vaddypally; Narasimha Reddy, Puram V.; Cronin, Leroy; Das, Samar K.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 20
• Pages of publication: 3781
• a: 11.844 ± 0.002 Å
• b: 11.01 ± 0.002 Å
• c: 22.643 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2952.7 ± 1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0342
• Residual factor for significantly intense reflections: 0.0329
• Weighted residual factors for significantly intense reflections: 0.0858
• Weighted residual factors for all reflections included in the refinement: 0.0867
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No