Information card for entry 7012125

Structure parameters

• Formula: C30 H33 Au6 Cl11.3 N12
• Calculated formula: C30 H33 Au6 Cl11.3 N12
• Title of publication: Oxidation of gold(i) pyrazolates by aqua regia. X-Ray crystal structures of the first examples of trinuclear AuIII3 and AuIAuIII2 pyrazolato complexes
• Authors of publication: Yang, Guang; Raptis, Raphael G.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 21
• Pages of publication: 3936
• a: 12.686 ± 0.003 Å
• b: 13.792 ± 0.003 Å
• c: 16.634 ± 0.003 Å
• α: 69.65 ± 0.03°
• β: 80.95 ± 0.03°
• γ: 67.6 ± 0.03°
• Cell volume: 2521.8 ± 1.2 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0747
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.084
• Weighted residual factors for all reflections included in the refinement: 0.0933
• Goodness-of-fit parameter for all reflections included in the refinement: 0.92
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No