Information card for entry 7012127

Structure parameters

• Formula: C15 H20 Au3 Cl2.22 N6
• Calculated formula: C15 H20 Au3 Cl2.22 N6
• Title of publication: Oxidation of gold(i) pyrazolates by aqua regia. X-Ray crystal structures of the first examples of trinuclear AuIII3 and AuIAuIII2 pyrazolato complexes
• Authors of publication: Yang, Guang; Raptis, Raphael G.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 21
• Pages of publication: 3936
• a: 23.92 ± 0.005 Å
• b: 11.8 ± 0.002 Å
• c: 7.74 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2184.7 ± 0.7 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.048
• Residual factor for significantly intense reflections: 0.0442
• Weighted residual factors for significantly intense reflections: 0.1079
• Weighted residual factors for all reflections included in the refinement: 0.1099
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No