Information card for entry 7012134

Structure parameters

• Common name: [Me2NCHNMe2][NiCl3(Me2NCH2NMe2)]
• Formula: C10 H27 Cl3 N4 Ni
• Calculated formula: C10 H27 Cl3 N4 Ni
• SMILES: [Ni]1(Cl)(Cl)(Cl)[N](C)(C)C[N]1(C)C.[N+](C)(C)=CN(C)C
• Title of publication: Anomalous reactions of the diamine Me2NCH2NMe2 with nickel(ii) and cobalt(ii)
• Authors of publication: Hitchcock, Peter B.; Handley, Darren A.; Huei Lee, Ting; Jeffery Leigh, G.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 24
• Pages of publication: 4720
• a: 15.257 ± 0.003 Å
• b: 7.922 ± 0.002 Å
• c: 15.488 ± 0.005 Å
• α: 90°
• β: 115.1 ± 0.02°
• γ: 90°
• Cell volume: 1695.2 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0469
• Residual factor for significantly intense reflections: 0.0369
• Weighted residual factors for significantly intense reflections: 0.0923
• Weighted residual factors for all reflections included in the refinement: 0.098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No