Information card for entry 7012137

Structure parameters

• Common name: [Ni3Cl4(OH)9tmeda)3][Ni3Cl4(OMe)(tmeda)3][NiCl3(tmeda)}2
• Formula: C41 H116 Cl14 N16 Ni8 O2
• Calculated formula: C41 H115 Cl14.234 N16 Ni8 O1.766
• Title of publication: Anomalous reactions of the diamine Me2NCH2NMe2 with nickel(ii) and cobalt(ii)
• Authors of publication: Hitchcock, Peter B.; Handley, Darren A.; Huei Lee, Ting; Jeffery Leigh, G.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 24
• Pages of publication: 4720
• a: 28.975 ± 0.005 Å
• b: 10.987 ± 0.002 Å
• c: 25.727 ± 0.004 Å
• α: 90°
• β: 102.266 ± 0.014°
• γ: 90°
• Cell volume: 8003 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0667
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.1136
• Weighted residual factors for all reflections included in the refinement: 0.1229
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No