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Information card for entry 7012158
Preview
Coordinates | 7012158.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H43 O5 Sb |
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Calculated formula | C24 H43 O5 Sb |
Title of publication | Antimony ??-diketonates and alkoxide/??-diketonates: remarkable formation of a 3,4-dihydro-2H-pyran ring by coupling of 1,1,1,5,5,5-hexafluoro-2,4-pentanedione ligands |
Authors of publication | Horley, Graeme A.; Mahon, Mary F.; Mazhar, Muhammed; Molloy, Kieran C.; Haycock, Peter W.; Myers, Christopher P. |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2002 |
Journal issue | 23 |
Pages of publication | 4416 |
a | 26.498 ± 0.0005 Å |
b | 11.78 ± 0.0002 Å |
c | 18.343 ± 0.0003 Å |
α | 90° |
β | 107.583 ± 0.0011° |
γ | 90° |
Cell volume | 5458.2 ± 0.17 Å3 |
Cell temperature | 170 ± 2 K |
Ambient diffraction temperature | 170 ± 2 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0558 |
Residual factor for significantly intense reflections | 0.0353 |
Weighted residual factors for significantly intense reflections | 0.1011 |
Weighted residual factors for all reflections included in the refinement | 0.1219 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.755 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7012158.html
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