Information card for entry 7012164

Structure parameters

• Formula: C15 H15 N O12 Os4
• Calculated formula: C15 H15 N O12 Os4
• Title of publication: Tetraosmium carbonyl clusters containing µ-NH2 amido ligands: syntheses, crystal structures and reactivities
• Authors of publication: Li, Yat; Wong, Wing-Tak
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 3
• Pages of publication: 398
• a: 15.986 ± 0.001 Å
• b: 17.119 ± 0.001 Å
• c: 17.981 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4920.8 ± 0.5 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for significantly intense reflections: 0.0583
• Weighted residual factors for all reflections included in the refinement: 0.0514
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No