Information card for entry 7012169

Structure parameters

• Formula: C9 H4 Br N O9 Os3
• Calculated formula: C9 H4 Br N O9 Os3
• Title of publication: Tetraosmium carbonyl clusters containing µ-NH2 amido ligands: syntheses, crystal structures and reactivities
• Authors of publication: Li, Yat; Wong, Wing-Tak
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 3
• Pages of publication: 398
• a: 13.392 ± 0.001 Å
• b: 9.762 ± 0.0006 Å
• c: 14.773 ± 0.001 Å
• α: 90°
• β: 113.96 ± 0.01°
• γ: 90°
• Cell volume: 1764.9 ± 0.2 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0353
• Weighted residual factors for all reflections included in the refinement: 0.0457
• Goodness-of-fit parameter for all reflections included in the refinement: 1.303
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No