Information card for entry 7012204

Structure parameters

• Formula: C80 H64 Ag6 N16 O40 P V3 W9
• Calculated formula: C80 H64 Ag6 N16 O40 P V3 W9
• Title of publication: A new α-Keggin type polyoxometalate coordinated to four silver complex moieties: {PW9V3O40[Ag(2,2'-bipy)]2[Ag2(2,2'-bipy)3]2}Electronic supplementary information (ESI) available: thermal ellipsoid plot of [Ag2(2,2'-bipy)3]2+, schematic representation of the molecular building blocks of 1, simplified 2-D representation of the supramolecular network of 1, IR spectra, XPS spectra and a TG curve for 1. See http://www.rsc.org/suppdata/dt/b2/b208531c/
• Authors of publication: Luan, Guoyou; Li, Yangguang; Wang, Shutao; Wang, Enbo; Han, Zhengbo; Hu, Changwen; Hu, Ninghai; Jia, Hengqing
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 2
• Pages of publication: 233
• a: 13.541 ± 0.003 Å
• b: 13.702 ± 0.003 Å
• c: 14.408 ± 0.003 Å
• α: 69.6 ± 0.03°
• β: 73.61 ± 0.03°
• γ: 83.27 ± 0.03°
• Cell volume: 2403.2 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.064
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for significantly intense reflections: 0.1183
• Weighted residual factors for all reflections included in the refinement: 0.1245
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No