Information card for entry 7012208

Structure parameters

• Formula: C16 H16 Cl3 N O2 P Rh
• Calculated formula: C16 H15 Cl3 N O2 P Rh
• Title of publication: Rhodium complexes containing the hybrid P,O ligand PPh2NHC(O)Me or its anion, [PPh2NC(O)Me]‒
• Authors of publication: Braunstein, Pierre; Heaton, Brian T.; Jacob, Chacko; Manzi, Lucia; Morise, Xavier
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 7
• Pages of publication: 1396 - 1401
• a: 9.5442 ± 0.0002 Å
• b: 16.4222 ± 0.0004 Å
• c: 13.2981 ± 0.0002 Å
• α: 90°
• β: 102.916 ± 0.009°
• γ: 90°
• Cell volume: 2031.57 ± 0.1 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.062
• Residual factor for significantly intense reflections: 0.053
• Weighted residual factors for all reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.07
• Goodness-of-fit parameter for all reflections: 1.037
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No