Information card for entry 7012228

Structure parameters

• Formula: C32 H36.4 Cl2 Ni2 O0.2 P2 S2
• Calculated formula: C32 H36 Cl2 Ni2 O0.2 P2 S2
• Title of publication: Synthesis of Ni(ii), Pd(ii) and Pt(ii) complexes containing chiral phosphino-thiol and -thioether ligands
• Authors of publication: Dervisi, Athanasia; Jenkins, Robert L.; Malik, K. M. Abdul; Hursthouse, Michael B.; Coles, Simon
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 6
• Pages of publication: 1133
• a: 11.523 ± 0.002 Å
• b: 12.031 ± 0.002 Å
• c: 13.325 ± 0.003 Å
• α: 76.37 ± 0.03°
• β: 79.93 ± 0.03°
• γ: 65.29 ± 0.03°
• Cell volume: 1624.8 ± 0.7 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0409
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.0701
• Weighted residual factors for all reflections included in the refinement: 0.0737
• Goodness-of-fit parameter for all reflections included in the refinement: 1.114
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No