Information card for entry 7012295

Structure parameters

• Common name: 01sot044
• Formula: C31 H33 Cl2 N5 Pd
• Calculated formula: C31 H33 Cl2 N5 Pd
• Title of publication: Chelating and 'pincer' dicarbene complexes of palladium; synthesis and structural studiesElectronic supplementary information (ESI) available: crystallographic data and ORTEP plot for compound 5c. See http://www.rsc.org/suppdata/dt/b2/b209739g/
• Authors of publication: Danopoulos, Andreas A.; Tulloch, Arran A. D.; Winston, Scott; Eastham, Graham; Hursthouse, Michael B.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 5
• Pages of publication: 1009
• a: 10.823 ± 0.002 Å
• b: 20.571 ± 0.004 Å
• c: 19.286 ± 0.004 Å
• α: 90°
• β: 90.86 ± 0.03°
• γ: 90°
• Cell volume: 4293.4 ± 1.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1255
• Residual factor for significantly intense reflections: 0.086
• Weighted residual factors for significantly intense reflections: 0.2334
• Weighted residual factors for all reflections included in the refinement: 0.2511
• Goodness-of-fit parameter for all reflections included in the refinement: 0.982
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No