Information card for entry 7012395

Structure parameters

• Formula: C21 H30 Cl N8 O Re S2
• Calculated formula: C21 H30 Cl N8 O Re S2
• Title of publication: Synthesis and characterisation of new homoleptic rhenium thiosemicarbazone complexes
• Authors of publication: Cowley, Andrew R.; Dilworth, Jonathan R.; Donnelly, Paul S.; Woollard-Shore, John
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 4
• Pages of publication: 748
• a: 8.8775 ± 0.0002 Å
• b: 11.9729 ± 0.0002 Å
• c: 12.6197 ± 0.0003 Å
• α: 96.4542 ± 0.0011°
• β: 93.2383 ± 0.0011°
• γ: 103.16 ± 0.0009°
• Cell volume: 1293.16 ± 0.05 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0268
• Weighted residual factors for all reflections included in the refinement: 0.0316
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9856
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No