Information card for entry 7012448

Structure parameters

• Formula: C50 H44 Ag2 B2 F8 N8 O2
• Calculated formula: C50 H40 Ag2 B2 F8 N8 O2
• Title of publication: The effect of phenyl substituents on supramolecular assemblies containing directly linked bis-pyridylimine ligands: synthesis and structural characterisation of mononuclear nickel(ii) and dinuclear silver(i) and cobalt(iii) complexes of (2-pyridyl)phenylketazine
• Authors of publication: Tuna, Floriana; Clarkson, Guy; Alcock, Nathaniel W.; Hannon, Michael J.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 11
• Pages of publication: 2149
• a: 20.445 ± 0.0016 Å
• b: 15.335 ± 0.0011 Å
• c: 32.547 ± 0.003 Å
• α: 90°
• β: 105.053 ± 0.002°
• γ: 90°
• Cell volume: 9854.1 ± 1.4 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1802
• Residual factor for significantly intense reflections: 0.0754
• Weighted residual factors for significantly intense reflections: 0.1388
• Weighted residual factors for all reflections included in the refinement: 0.1758
• Goodness-of-fit parameter for all reflections included in the refinement: 0.984
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No