Information card for entry 7012559

Structure parameters

• Formula: C78.3 H66.3 B2 Cl14.9 F8 Fe2 N2 O2 P4 Ru2
• Calculated formula: C39.15 H33.15 B Cl7.45 F4 Fe N O P2 Ru
• Title of publication: Synthesis, structure and reactions of coordinatively unsaturated [RuCl(CO)(dppf)(PPh3)]BF4 where dppf is trans-spanning 1,1'-bis(diphenylphosphino)ferrocene
• Authors of publication: Kawano, Hiroyuki; Nishimura, Yoshimasa; Onishi, Masayoshi
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 9
• Pages of publication: 1808
• a: 12.363 ± 0.001 Å
• b: 13.627 ± 0.002 Å
• c: 14.457 ± 0.002 Å
• α: 99.377 ± 0.005°
• β: 110.241 ± 0.001°
• γ: 93.587 ± 0.002°
• Cell volume: 2236 ± 0.5 ų
• Cell temperature: 296.2 K
• Number of distinct elements: 10
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0824
• Weighted residual factors for all reflections included in the refinement: 0.2584
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No