Information card for entry 7012705

Structure parameters

• Formula: C27 H37 Cl2 N3 O Pd3
• Calculated formula: C27 H37 Cl2 N3 O Pd3
• Title of publication: New phosphino-oxazoline and related phosphino-iminolate palladium complexes; structure of an unusual zwitterionic dinuclear Pd(ii) complex
• Authors of publication: Apfelbacher, Andreas; Braunstein, Pierre; Brissieux, Luc; Welter, Richard
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 9
• Pages of publication: 1669
• a: 9.54 ± 0.005 Å
• b: 12.37 ± 0.005 Å
• c: 13.327 ± 0.005 Å
• α: 84.288 ± 0.005°
• β: 82.088 ± 0.005°
• γ: 70.423 ± 0.005°
• Cell volume: 1465.3 ± 1.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0542
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.0917
• Weighted residual factors for all reflections included in the refinement: 0.0991
• Goodness-of-fit parameter for all reflections included in the refinement: 0.946
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No