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Information card for entry 7012730
Preview
Coordinates | 7012730.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | complex 15 |
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Formula | C33.5 H19 B Cl7.5 D1.5 F10 N3 Zr |
Calculated formula | C33.5 H20.4085 B Cl7.5 F10 N3 Zr |
Title of publication | The synthesis of half-sandwich bis(pentafluorophenyl)boryl-substituted cyclopentadienyl zirconium, niobium and tantalum complexes and the isolation and molecular structure of a zwitterionic niobocene |
Authors of publication | Lancaster, Simon J.; Hughes, David L. |
Journal of publication | Dalton Transactions |
Year of publication | 2003 |
Journal issue | 9 |
Pages of publication | 1779 |
a | 11.201 ± 0.001 Å |
b | 18.241 ± 0.001 Å |
c | 21.174 ± 0.003 Å |
α | 67.46 ± 0.01° |
β | 76.82 ± 0.01° |
γ | 84.93 ± 0.01° |
Cell volume | 3890.5 ± 0.8 Å3 |
Cell temperature | 140 ± 1 K |
Ambient diffraction temperature | 140 ± 1 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0424 |
Residual factor for significantly intense reflections | 0.0366 |
Weighted residual factors for significantly intense reflections | 0.0974 |
Weighted residual factors for all reflections included in the refinement | 0.1004 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | Mo-Kα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7012730.html
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