Information card for entry 7012742

Structure parameters

• Formula: C32 H36 N2 P2
• Calculated formula: C32 H36 N2 P2
• Title of publication: Novel chiral 1,5-diaza-3,7-diphosphacyclooctane ligands and their transition metal complexes
• Authors of publication: Andrey A. Karasik; Roman N. Naumov; Oleg G. Sinyashin; Gennadii P. Belov; Helena V. Novikova; Peter Lönnecke; Evamarie Hey-Hawkins
• Journal of publication: Dalton Trans.
• Year of publication: 2003
• Journal issue: 11
• Pages of publication: 2209 - 2214
• a: 23.052 ± 0.012 Å
• b: 5.472 ± 0.003 Å
• c: 22.567 ± 0.012 Å
• α: 90°
• β: 100.552 ± 0.01°
• γ: 90°
• Cell volume: 2798 ± 3 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 4
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.1378
• Residual factor for significantly intense reflections: 0.0718
• Weighted residual factors for significantly intense reflections: 0.1428
• Weighted residual factors for all reflections included in the refinement: 0.1758
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No