Crystallography Open Database

Information card for entry 7012746

Preview

Coordinates	7012746.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C45 H53 O4 Rh2 Sb
Calculated formula	C45 H53 O4 Rh2 Sb
SMILES	C1(c2ccccc2)(c2ccccc2)[Rh]234(C(c5ccccc5)(c5ccccc5)[Rh]514([O]=C(C)O5)[Sb]3(C(C)C)(C(C)C)C(C)C)[O]=C(C)O2.c1ccccc1
Title of publication	A series of di-nuclear rhodium(i) complexes with trialkylstibines as bridging ligands
Authors of publication	Pechmann, Thomas; Brandt, Carsten D.; Werner, Helmut
Journal of publication	Dalton Transactions
Year of publication	2003
Journal issue	8
Pages of publication	1495 - 1499
a	19.0176 ± 0.001 Å
b	20.0618 ± 0.0011 Å
c	11.0473 ± 0.0006 Å
α	90°
β	103.36 ± 0.001°
γ	90°
Cell volume	4100.8 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0246
Residual factor for significantly intense reflections	0.0237
Weighted residual factors for significantly intense reflections	0.0572
Weighted residual factors for all reflections included in the refinement	0.0577
Goodness-of-fit parameter for all reflections included in the refinement	1.172
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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