Information card for entry 7012748

Structure parameters

• Chemical name: (Trimethylsilyl)-bis[(trimethylsilyl)imino-(phenyl)methyl]digermane
• Formula: C46 H74 Ge2 N4 Si6
• Calculated formula: C46 H74 Ge2 N4 Si6
• SMILES: C[Si](C)([Ge](C(=N\[Si](C)(C)C)\c1ccccc1)(/C(c1ccccc1)=N/[Si](C)(C)C)[Ge](/C(c1ccccc1)=N/[Si](C)(C)C)(/C(=N/[Si](C)(C)C)c1ccccc1)[Si](C)(C)C)C
• Title of publication: Synthesis, crystal structures and reactions of sila- and germa-β-diketiminates
• Authors of publication: Farwell, James D.; Fernandes, Manuel A.; Hitchcock, Peter B.; Lappert, Michael F.; Layh, Marcus; Omondi, Bernard
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 9
• Pages of publication: 1719
• a: 10.2204 ± 0.0013 Å
• b: 12.0349 ± 0.0015 Å
• c: 13.3254 ± 0.0017 Å
• α: 114.225 ± 0.002°
• β: 109.868 ± 0.002°
• γ: 92.296 ± 0.002°
• Cell volume: 1374.6 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0469
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.1093
• Weighted residual factors for all reflections included in the refinement: 0.1102
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No