Information card for entry 7012815

Structure parameters

• Formula: C39 H94 F6 O3.5 P6 Ru2 S
• Calculated formula: C39 H94 F6 O3.5 P6 Ru2 S
• Title of publication: Replacement of [RuH2(PMe3)4] by [RuH2(PEt3)4] switches reaction products: synthesis of fluoride-bridged diruthenium complexes
• Authors of publication: Jasim, Naseralla A.; Perutz, Robin N.; Archibald, Stephen J.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 11
• Pages of publication: 2184
• a: 14.89 ± 0.0014 Å
• b: 19.3584 ± 0.0017 Å
• c: 21.205 ± 0.002 Å
• α: 106.41 ± 0.007°
• β: 106.8 ± 0.007°
• γ: 103.127 ± 0.007°
• Cell volume: 5286.3 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1017
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.1141
• Weighted residual factors for all reflections included in the refinement: 0.1267
• Goodness-of-fit parameter for all reflections included in the refinement: 0.827
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No