Information card for entry 7012922

Structure parameters

• Formula: C30 H86 K2 N4 O6 Si6 Zn2
• Calculated formula: C30 H86 K2 N4 O6 Si6 Zn2
• Title of publication: Facile synthesis and structural variation of novel heterobimetallic alkali metal?zinc-alkoxide and -siloxide clustersElectronic supplementary information (ESI) available: the ESI spectra of the reaction mixtures tBuOLi + ZnMe2, Me3SiOK + ZnMe2 and tBuOK + ZnMe2. See http://www.rsc.org/suppdata/dt/b3/b302585c/
• Authors of publication: Merz, Klaus; Block, Stefan; Schoenen, Robert; Driess, Matthias
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 17
• Pages of publication: 3365
• a: 19.208 ± 0.007 Å
• b: 10.995 ± 0.004 Å
• c: 13.369 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2823.4 ± 1.8 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 7
• Space group number: 58
• Hermann-Mauguin space group symbol: P n n m
• Hall space group symbol: -P 2 2n
• Residual factor for all reflections: 0.0873
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.1228
• Weighted residual factors for all reflections included in the refinement: 0.146
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No