Information card for entry 7012938

Structure parameters

• Formula: C91 H101 Cl4 N9 O4 U
• Calculated formula: C92 H99 Cl4 N8 O4 U
• Title of publication: Complexes of uranium(IV) with acyclic polyphenoxides resulting from cleavage of homooxacalixarenes
• Authors of publication: Lionel Salmon; Pierre Thuéry; Michel Ephritikhine; Bernardo Masci
• Journal of publication: Dalton Trans.
• Year of publication: 2003
• Journal issue: 12
• Pages of publication: 2405 - 2410
• a: 30.39 ± 0.003 Å
• b: 15.5898 ± 0.0016 Å
• c: 20.2637 ± 0.0011 Å
• α: 90°
• β: 112.651 ± 0.005°
• γ: 90°
• Cell volume: 8859.9 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1831
• Residual factor for significantly intense reflections: 0.0848
• Weighted residual factors for significantly intense reflections: 0.1726
• Weighted residual factors for all reflections included in the refinement: 0.2278
• Goodness-of-fit parameter for all reflections included in the refinement: 0.95
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No