Information card for entry 7012955

Structure parameters

• Formula: H108 N14 O96 Sb2 U2 W18
• Calculated formula: N14 O96 Sb2 U2 W18
• Title of publication: A new structural family of heteropolytungstate lacunary complexes with the uranyl, UO22+, cation
• Authors of publication: Gaunt, Andrew J.; May, Iain; Copping, Roy; Bhatt, Anand I.; Collison, David; Danny Fox, O.; Travis Holman, K.; Pope, Michael T.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 15
• Pages of publication: 3009
• a: 17.2397 ± 0.0018 Å
• b: 11.5314 ± 0.0012 Å
• c: 47.816 ± 0.005 Å
• α: 90°
• β: 99.757 ± 0.002°
• γ: 90°
• Cell volume: 9368.2 ± 1.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.054
• Residual factor for significantly intense reflections: 0.0403
• Weighted residual factors for significantly intense reflections: 0.0813
• Weighted residual factors for all reflections included in the refinement: 0.0856
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No