Information card for entry 7013004

Structure parameters

• Common name: 1
• Formula: C19 H34 Ag2 B22 Br2 Cl2 I2 Mo2 O6
• Calculated formula: C19 H34 Ag2 B22 Br2 Cl2 I2 Mo2 O6
• Title of publication: Investigation of the synthesis of {Mo(η5-C5H5)(CO)3}+ fragments partnered with the monoanionic carboranes [closo-CB11H11Br]-, [closo-CB11H6Br6]- and [closo-HCB11Me11]- by silver salt metathesis and hydride abstraction
• Authors of publication: Patmore, Nathan J.; Ingleson, Michael J.; Mahon, Mary F.; Weller, Andrew S.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 14
• Pages of publication: 2894 - 2904
• a: 12.779 ± 0.003 Å
• b: 13.53 ± 0.003 Å
• c: 13.725 ± 0.003 Å
• α: 99.47 ± 0.03°
• β: 101.09 ± 0.03°
• γ: 98.31 ± 0.03°
• Cell volume: 2258.6 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.038
• Residual factor for significantly intense reflections: 0.0294
• Weighted residual factors for significantly intense reflections: 0.0635
• Weighted residual factors for all reflections included in the refinement: 0.067
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No