Information card for entry 7013013

Structure parameters

• Formula: C72 H114 Cl2 Mg2 N4
• Calculated formula: C74 H115 Cl2 Mg2 N4
• Title of publication: Low coordinate magnesium chemistry supported by a bulky ?-diketiminate ligand
• Authors of publication: Dove, Andrew P.; Gibson, Vernon C.; Hormnirun, Pimpa; Marshall, Edward L.; Segal, John A.; White, Andrew J. P.; Williams, David J.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 15
• Pages of publication: 3088
• a: 12.2182 ± 0.0003 Å
• b: 17.9539 ± 0.001 Å
• c: 16.4195 ± 0.0006 Å
• α: 90°
• β: 97.653 ± 0.002°
• γ: 90°
• Cell volume: 3569.8 ± 0.3 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: I 1 2/m 1
• Hall space group symbol: -I 2y
• Residual factor for all reflections: 0.0596
• Residual factor for significantly intense reflections: 0.047
• Weighted residual factors for all reflections: 0.1317
• Weighted residual factors for significantly intense reflections: 0.1174
• Goodness-of-fit parameter for all reflections: 1.073
• Goodness-of-fit parameter for significantly intense reflections: 1.092
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No