Information card for entry 7013030

Structure parameters

• Formula: C30 H35 Cl2 N6 O0.25 P Rh
• Calculated formula: C30 H34 Cl2 N6 O0.25 P Rh
• Title of publication: Synthesis and coordination chemistry of aminophosphine derivatives of adenineElectronic supplementary information (ESI) available: Preparation of all compounds apart from L1 and complex 11; Tables S1?S8: NMR spectral data of all the compounds. See http://www.rsc.org/suppdata/dt/b3/b303715k
• Authors of publication: Zhang, Qingzhi; Hua, Guoxiong; Bhattacharyya, Pravat; Slawin, Alexandra M. Z.; Derek Woollins, J.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 16
• Pages of publication: 3250
• a: 16.31 ± 0.0002 Å
• b: 9.0989 ± 0.0001 Å
• c: 22.2647 ± 0.0002 Å
• α: 90°
• β: 96.689 ± 0.001°
• γ: 90°
• Cell volume: 3281.66 ± 0.06 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.049
• Residual factor for significantly intense reflections: 0.0369
• Weighted residual factors for significantly intense reflections: 0.0995
• Weighted residual factors for all reflections included in the refinement: 0.1062
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No