Crystallography Open Database

Information card for entry 7013090

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Coordinates	7013090.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H40 Cl4 N6 Ru
Calculated formula	C24 H40 Cl4 N6 Ru
Title of publication	The formation of cis- and trans-[Ru(CN)2(CNtBu)4] by reductive cleavage of isocyanide ligands; isomer separation by supramolecular interactions with various solvents
Authors of publication	Daniel Dönnecke; Wolfgang Imhof
Journal of publication	Dalton Trans.
Year of publication	2003
Journal issue	13
Pages of publication	2737 - 2744
a	34.673 ± 0.007 Å
b	10.0852 ± 0.0012 Å
c	19.288 ± 0.002 Å
α	90°
β	92.205 ± 0.008°
γ	90°
Cell volume	6739.7 ± 1.7 Å³
Cell temperature	183 ± 2 K
Ambient diffraction temperature	183 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0404
Residual factor for significantly intense reflections	0.0348
Weighted residual factors for all reflections	0.0948
Weighted residual factors for significantly intense reflections	0.0853
Goodness-of-fit parameter for all reflections	1.075
Goodness-of-fit parameter for significantly intense reflections	1.08
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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