Information card for entry 7013153

Structure parameters

• Formula: C36 H46 Cl2 N4 O7 Os
• Calculated formula: C36 H44 Cl2 N4 O7 Os
• SMILES: [Os]123(Oc4c(cccc4)C(=O)N2c2c(N3C(=O)C3=C(O1)C(=O)C=CC3=O)cc(Cl)c(Cl)c2)#N.O.[N+](CCCC)(CCCC)(CCCC)CCCC
• Title of publication: Nitrido-ruthenium(vi) and -osmium(vi) complexes of multianionic chelating (N, O) ligands. Reactions with nucleophiles, electrophiles and oxidizing agentsElectronic supplementary information (ESI) available: Fig. S1?S6. See http://www.rsc.org/suppdata/dt/b3/b304920p/
• Authors of publication: Yip, Ka-Lai; Yu, Wing-Yiu; Chan, Pui-Ming; Zhu, Nian-Yong; Che, Chi-Ming
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 3556
• a: 13.732 ± 0.003 Å
• b: 18.256 ± 0.004 Å
• c: 15.546 ± 0.003 Å
• α: 90°
• β: 99.81 ± 0.03°
• γ: 90°
• Cell volume: 3840.3 ± 1.4 ų
• Cell temperature: 301 ± 2 K
• Ambient diffraction temperature: 301 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0864
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.0974
• Weighted residual factors for all reflections included in the refinement: 0.1397
• Goodness-of-fit parameter for all reflections included in the refinement: 0.963
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No