Information card for entry 7013192

Structure parameters

• Formula: C31.8 H38.4 Cl3 Co N O1.4 P2
• Calculated formula: C31.8 H38 Cl3 Co N O1.4 P2
• Title of publication: Tetrahedral cobalt(ii) complexes stabilized by the aminodiphosphine PNP ligand [PNP = CH3CH2CH2N(CH2CH2PPh2)2]
• Authors of publication: Romerosa, Antonio; Saraiba-Bello, Cristobal; Serrano-Ruiz, Manuel; Caneschi, Andrea; McKee, Vickie; Peruzzini, Maurizio; Sorace, Lorenzo; Zanobini, Fabrizio
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 16
• Pages of publication: 3233
• a: 29.86 ± 0.005 Å
• b: 13.108 ± 0.002 Å
• c: 22.394 ± 0.004 Å
• α: 90°
• β: 130.973 ± 0.002°
• γ: 90°
• Cell volume: 6617.8 ± 1.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1223
• Residual factor for significantly intense reflections: 0.0755
• Weighted residual factors for significantly intense reflections: 0.2048
• Weighted residual factors for all reflections included in the refinement: 0.2384
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No