Information card for entry 7013224

Structure parameters

• Common name: dichloro(5,7-hydroxy-6-oxo-1,4,8,11-tetraazacyclotetradecane- 5,7-diene)cobalt(
• Chemical name: dichloro(5,7-hydroxy-6-oxo-1,4,8,11-tetraazacyclotetradecane-5,7- diene)cobalt(
• Formula: C10 H17 Cl2 Co N4 O3.5
• Calculated formula: C10 H17 Cl2 Co N4 O3.5
• Title of publication: Synthesis, structural studies and photochemistry of cobalt(iii) complexes of anthracenylcyclam macrocyclesElectronic supplementary information (ESI) available: Selected bond lengths and angles and ORTEP diagrams for compound 8 and complexes [Co(3)Cl2]Cl�4H2O, [Co(12)Cl2] and [Co(2)Cl2]Cl�0.5CH3OH. See http://www.rsc.org/suppdata/dt/b3/b305773a/
• Authors of publication: Funston, Alison M.; Ghiggino, Kenneth P.; Grannas, Martin J.; David McFadyen, W.; Tregloan, Peter A.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 19
• Pages of publication: 3704
• a: 10.0111 ± 0.0011 Å
• b: 14.891 ± 0.003 Å
• c: 9.692 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1444.8 ± 0.4 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 6
• Space group number: 58
• Hermann-Mauguin space group symbol: P n n m
• Hall space group symbol: -P 2 2n
• Residual factor for all reflections: 0.1199
• Residual factor for significantly intense reflections: 0.0854
• Weighted residual factors for significantly intense reflections: 0.2246
• Weighted residual factors for all reflections included in the refinement: 0.2472
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No