Information card for entry 7013515

Structure parameters

• Formula: C20 H52 Cu4 N4 O28 P4
• Calculated formula: C20 H52 Cu4 N4 O28 P4
• Title of publication: Synthesis, structure and magnetic properties of [Cu4(Hmbpp)2(H2NC(O)NH2)2(H2O)8]�4H2O
• Authors of publication: Harrison, Andrew; Henderson, David K.; Lovatt, Paul A.; Parkin, Andrew; Tasker, Peter A.; Winpenny, Richard E. P.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 22
• Pages of publication: 4271
• a: 7.9478 ± 0.0018 Å
• b: 14.715 ± 0.003 Å
• c: 17.977 ± 0.004 Å
• α: 90°
• β: 99.129 ± 0.004°
• γ: 90°
• Cell volume: 2075.8 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0249
• Residual factor for significantly intense reflections: 0.0227
• Weighted residual factors for significantly intense reflections: 0.0659
• Weighted residual factors for all reflections included in the refinement: 0.0665
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No