Information card for entry 7013547

Structure parameters

• Formula: C20 H15 Cl N2 O P Rh
• Calculated formula: C20 H15 Cl N2 O P Rh
• SMILES: [Rh]1([P](n2c3[n]1cccc3cc2)(c1ccccc1)c1ccccc1)(Cl)C#[O]
• Title of publication: The synthesis and late transition metal chemistry of 7-aza-N-indolyl phosphines and the activity of their palladium complexes in CO?ethene co-polymerisation
• Authors of publication: Burrows, Andrew D.; Mahon, Mary F.; Varrone, Maurizio
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 24
• Pages of publication: 4718
• a: 9.002 ± 0.0002 Å
• b: 13.836 ± 0.0004 Å
• c: 15.009 ± 0.0004 Å
• α: 85.766 ± 0.0011°
• β: 82.966 ± 0.0011°
• γ: 87.527 ± 0.0014°
• Cell volume: 1849.16 ± 0.08 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0526
• Residual factor for significantly intense reflections: 0.0404
• Weighted residual factors for significantly intense reflections: 0.0959
• Weighted residual factors for all reflections included in the refinement: 0.1033
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No