Information card for entry 7013634

Structure parameters

• Formula: C35.5 H31 Cl F6 N2 O P2 Pd
• Calculated formula: C35.5 H31 Cl F6 N2 O P2 Pd
• Title of publication: Synthesis and characterisation of cyclometallated palladium(II) complexes with phosphine‒carboxylate and phosphine‒amide ligands
• Authors of publication: Gregorio Sánchez; Joaquín García; David Meseguer; José L. Serrano; Luis García; José Pérez; Gregorio López
• Journal of publication: Dalton Trans.
• Year of publication: 2003
• Journal issue: 24
• Pages of publication: 4709 - 4717
• a: 9.1497 ± 0.0006 Å
• b: 13.4993 ± 0.0008 Å
• c: 13.9376 ± 0.0008 Å
• α: 89.88 ± 0.004°
• β: 82.8 ± 0.006°
• γ: 77.079 ± 0.005°
• Cell volume: 1664.08 ± 0.18 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0538
• Residual factor for significantly intense reflections: 0.0431
• Weighted residual factors for significantly intense reflections: 0.1165
• Weighted residual factors for all reflections included in the refinement: 0.1425
• Goodness-of-fit parameter for all reflections included in the refinement: 1.172
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No