Information card for entry 7013796

Structure parameters

• Formula: C31 H33 I2 O0.67 P Rh2
• Calculated formula: C31.0067 H33.02 I2 O0.66 P Rh2
• Title of publication: Extending the coordination capabilities of tertiary phosphines and arsines: preparation, molecular structure, and reactivity of dinuclear rhodium complexes with PR3 and AsR3 in a doubly bridging coordination mode.
• Authors of publication: Pechmann, Thomas; Brandt, Carsten D.; Werner, Helmut
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 6
• Pages of publication: 959 - 966
• a: 22.9416 ± 0.0017 Å
• b: 22.9416 ± 0.0017 Å
• c: 31.23 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 14235 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 167
• Hermann-Mauguin space group symbol: R -3 c :H
• Hall space group symbol: -R 3 2"c
• Residual factor for all reflections: 0.0649
• Residual factor for significantly intense reflections: 0.0643
• Weighted residual factors for significantly intense reflections: 0.1368
• Weighted residual factors for all reflections included in the refinement: 0.1371
• Goodness-of-fit parameter for all reflections included in the refinement: 1.337
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No