Information card for entry 7013892

Structure parameters

• Formula: C20 H40 Cl2 O18 Sm
• Calculated formula: C20 H40 Cl2 O18 Sm
• Title of publication: Two complexes of Sm(II) with crown ethers-electrochemical synthesis, structure and spectroscopy.
• Authors of publication: Starynowicz, Przemysław
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 5
• Pages of publication: 825 - 832
• a: 17.903 ± 0.009 Å
• b: 17.903 ± 0.009 Å
• c: 17.903 ± 0.009 Å
• α: 108.35 ± 0.06°
• β: 108.35 ± 0.06°
• γ: 108.35 ± 0.06°
• Cell volume: 4592 ± 6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 161
• Hermann-Mauguin space group symbol: R 3 c :R
• Hall space group symbol: P 3* -2n
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.0548
• Weighted residual factors for significantly intense reflections: 0.0726
• Weighted residual factors for all reflections included in the refinement: 0.0811
• Goodness-of-fit parameter for all reflections included in the refinement: 0.931
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No