Information card for entry 7014001

Structure parameters

• Formula: C39 H45 N Ni O P2
• Calculated formula: C39 H45 N Ni O P2
• Title of publication: Synthesis, characterization and ethylene reactivity of 2-diphenylphosphanylbenzamido nickel complexes.
• Authors of publication: Kwon, Heon Yong; Lee, Su Yeon; Lee, Bun Yeoul; Shin, Dong Mok; Chung, Young Keun
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 6
• Pages of publication: 921 - 928
• a: 24.636 ± 0.001 Å
• b: 13.792 ± 0.001 Å
• c: 21.955 ± 0.001 Å
• α: 90°
• β: 108.448 ± 0.002°
• γ: 90°
• Cell volume: 7076.5 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1625
• Residual factor for significantly intense reflections: 0.0715
• Weighted residual factors for significantly intense reflections: 0.1598
• Weighted residual factors for all reflections included in the refinement: 0.1969
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No