Information card for entry 7014008

Structure parameters

• Formula: C56 H60 Br6 Co4 N32 O12
• Calculated formula: C56 H52 Br6 Co4 N32 O9
• Title of publication: Self-assembled polynuclear clusters derived from some flexible polydentate dihydrazide ligands.
• Authors of publication: Zhao, Liang; Niel, Virginie; Thompson, Laurence K.; Xu, Zhiqiang; Milway, Victoria A.; Harvey, Rosemary G.; Miller, David O.; Wilson, Claire; Leech, Michael; Howard, Judith A. K.; Heath, Sarah L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 9
• Pages of publication: 1446 - 1455
• a: 32.664 ± 0.002 Å
• b: 17.8963 ± 0.0012 Å
• c: 35.999 ± 0.002 Å
• α: 90°
• β: 116.953 ± 0.001°
• γ: 90°
• Cell volume: 18758 ± 2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1089
• Residual factor for significantly intense reflections: 0.0605
• Weighted residual factors for significantly intense reflections: 0.1622
• Weighted residual factors for all reflections included in the refinement: 0.177
• Goodness-of-fit parameter for all reflections included in the refinement: 0.928
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No