Information card for entry 7014010

Structure parameters

• Formula: C30 H38 N10 Ni4 O18
• Calculated formula: C30 H37 N10 Ni4 O18
• Title of publication: Self-assembled polynuclear clusters derived from some flexible polydentate dihydrazide ligands.
• Authors of publication: Zhao, Liang; Niel, Virginie; Thompson, Laurence K.; Xu, Zhiqiang; Milway, Victoria A.; Harvey, Rosemary G.; Miller, David O.; Wilson, Claire; Leech, Michael; Howard, Judith A. K.; Heath, Sarah L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 9
• Pages of publication: 1446 - 1455
• a: 8.5023 ± 0.0006 Å
• b: 25.4503 ± 0.0018 Å
• c: 18.7049 ± 0.0014 Å
• α: 90°
• β: 99.805 ± 0.001°
• γ: 90°
• Cell volume: 3988.4 ± 0.5 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0676
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for significantly intense reflections: 0.1377
• Weighted residual factors for all reflections included in the refinement: 0.1469
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No